Characterization of isothermally oxidized ZrO2-8wt.%Y 2O3 thermal barrier coatings by electrochemical impedance spectroscopy

J. W. Byeon, B. Jayaraj, Y. H. Sohn

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

Abstract

Electrochemical impedance spectroscopy was employed to examine ZrO 2-8wt.%Y2O3 (yttria stabilized zirconia, YSZ) thermal barrier coating (TBC) as a function of isothermal exposure time at 1121°C. Electrochemical impedance response (resistance and capacitance of YSZ and thermally grown oxide (TGO)) of TBC specimens was analyzed with an alternative current equivalent circuit based on the multi-layered micro-constituents of TBC, and the impedance response was correlated with microstructural changes attributed to isothermal oxidation. The resistance of YSZ was observed to increase initially and then decrease with thermal exposure. The initial increase was related to the high temperature sintering of YSZ, and the subsequent decrease was discussed in terms of microcrack initiation and electrolyte penetration. The TGO thickness was linearly correlated to the capacitance of TGO.

Original languageEnglish
Title of host publicationEco-Materials Processing and Design VI - Proceedings of the 6th International Symposium on Eco-Materials Processing and Design, ISEPD-6
PublisherTrans Tech Publications Ltd
Pages145-148
Number of pages4
ISBN (Print)0878499660, 9780878499663
DOIs
StatePublished - 2005
Event6th International Symposium on Eco-Materials Processing and Design, ISEPD-6 - Jinju, Korea, Republic of
Duration: 16 Jan 200518 Jan 2005

Publication series

NameMaterials Science Forum
Volume486-487
ISSN (Print)0255-5476
ISSN (Electronic)1662-9752

Conference

Conference6th International Symposium on Eco-Materials Processing and Design, ISEPD-6
Country/TerritoryKorea, Republic of
CityJinju
Period16/01/0518/01/05

Keywords

  • Electrochemical impedance spectroscopy
  • Isothermal oxidation
  • Nondestructive evaluation
  • Thermal barrier coating
  • Thermally grown oxide

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